Skip to main content

Collection and preparation of soil and water samples for analsis

Sampling Equipments-
  Spade, screw auger (depth wise) or post-hole auger (for moist soil), khudali (pick axe), khurpi, trowel, steel spatula clean plastic bucket, plastic container, cloth bag, information sheet, scale for measuring pit depth marking pencil. 

How to collect the soil sample 
  • Remove or scrap the upper portion  or surface of the soil and remove the crop residues and litters which is on the soil surface.
  • Take pick axe (khudali) and spad with spatula and dig out near about 15-20 cm deep soil width khudali or picking axe. The shape should be V shaped. Remove and reject first digged surface soil. Then collect the soil in the plastic paper or container from selected spots in the field. 
  • Mix all the soil which is taken from different spots in the plastic paper or container. 
  • Avoid soil sampling where  fertilizer and manure applied recently. After mixing the soil sample divide it in four part. Then reject two part form quarter and  take remaining two parts of soil from the plastic  paper  or container .
  • Minimum we have to take 1/2 kg or 1kg soil sample for analysis write the information which is given in sheet.                            
  •   Sample preparation
Drying - Mixed the soil uniformly and spread the soil on polythene for air drying for about 4-5 days in a well-ventilated room of shed.
Grinding -use a mortar and pestle to grind the sample. The grinding breaks down aggregates and mixes the sample. 
Sieving -At least 2mm sieve should be used for sieving soil. Avoid micronutrient contamination do not use a brass, copper or galvanized iron sieve.                                           Technique for  water  sampling -
  • Common sampling tool and accessories. 
  • Clean plastic glass bottles of 500ml capacity. 
Cotton or nylon thread, glass marking pencil and labels  and tags. 

Water  sample collection procedure -
Clean the container before the use and rinsed 3 to 4 times with the water. 
If the source of irritation water is tank,canal or river,  the water sample should be drawn either from a spot, away from the sides or from the midstream with the help of bucket.  The tube well and hand pump are to be run for 10-20 minutes  prior  to, sampling and for open well, several buckets of water have to be thrown out first. About half a liter of the sample is quite sufficient. 
If delay for testing. Add 1 to 3 drops of pure toluene to prevent the bacterial activity. Fill the water sample in the plastic bottles labeled them and sent to laboratory immediately for testing so as to avoid any changes or deterioration in its quality due to the chemical  or microbial activity. 

Comments

Popular posts from this blog

ORGANIC CARBON IN SOIL - DETERMINATION BY WALKLEY & BLACK METHOD.

TITLE :- Determination of organic carbon in soil by walkley & black method.  Principle -   The organic carbon in organic matter is oxidised by known excess of chromic acid .(K2 cr2 O7 + H2 s o4). The excess acid chromic acid not reduced by organic matter is determined by Black titration which standard feso4 solution (redox titration) using ferroin indicator. the organic in soil calculated from the chromic acid utilised (reduced by it) Reagent  Potassium dichromate solutions,  Dissolve 49.04gm of dried reagents grade potassium dichromate, K2cr2O7 in distilled water & dilute it to one liter.  Ferrous sulphate solutions 0.5N Dissolve 139gm of reagent grade ferrous sulphate feso4. 7H2o in distilled  water and add 15ml of concentrated H2so4 cool and dilute to one litters or dissolve 196.19gm ferrous  ammonium sulphate feso4(NH4)so4.6H2o and making up-to one litters standardized the solution against potassium add 20 ml concentrated H2so4, before making 1 liter  volume.  Ferroin indic

Determination of CLORIDES from irrigation water sample.

Aim - Determination of chloride from irrigation water simple.  Principle - Mohr's titration method (argentrometric) is most commonly used for chlorides determination.  It Depend upon formation of sparingly soluble greek silver chromate (AgcrO4) precipitated at the end point.  When sample is titrated against the standard Silver Nitrate (AgNo3) solution in presence of potassium chromate (k2crO4) as colour indicator. Reagents - 1) potassium chromate indicator 5% solution - Dissolved 5gm potassium chromate in about 75 distilled water and add saturated solution of silver nitrate. Dropwise until a slite permanent red precipitated is formed. Filter and dilute 100ml with distilled water . 2) standard silver nitrate (0.02 normality AgNo3) - Dissolved 3.40 gram silver nitrate in distilled water and volume made up to 1 litre and stored in Amber colour bottle away from light.  Procedure - Take 10 ml of water sample in hundred ml conical flask and dilute to 25 ml with distilled water.  Add 5 dr

Determination of available potassium from soil.

TITLE - Detemination of available potassium from soil.  REAGENTS  -  1) Neutral ammonium acetate - Dissolved 77.1 gram ammonium acetate 900 ml water & adjust the pH to 7 by Acetic Acid or Ammonium hydroxide dilute to 1 litre. 2) preparation of standad solution.- Dissolved 1.908 gram KCL in distal water. And makeup the final volume one litre. this solution called as stock solution. 3)  Preparation working solution. - Take 10 ml solution from stock solution and makeup volume 100 ml. 4) Preparation of standard series - Prepare 0 2 4 6 8 10 ml of working solution **** PROCEDURES  - 1) Take 5 gram of soil in conical flask. 2) Add 25 ml of neutral normal            ammonium acetate.  3) Shake for 5 minut. 4) Filter the content.  5) Take reading on flame photometer. GRAPH FACTOR Graph factor reading            Flame Concentration.                      Photometer                                                   Reading.  0                              -             2